With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.134030-21-0,N1,N2-Dimesitylethane-1,2-diamine,as a common compound, the synthetic route is as follows.
In a GPC bottle, N,N?- dimesityl-ethanediamine (2 mmol) and C6F5CHO (3 mmol) were introduced. The mixture was crushed with a glass rod and a few drops of glacial acetic acid were added while stirring. After adding glacial acetic acid (1 mL) a precipitate was formed. Another glacial acetic acid (1 mL) was added, and the precipitate obtained after filtration was washed with cold isopropanol (-20 C) and then dried. The product was obtained as a white powder. Yield: 0.34g, 35%. 1H NMR (250 MHz, CDCl3) delta 6.79 (s, 4H), 6.37 (s, 1H), 3.89 (m, 2H), 3.51 (m, 2H), 2.51 (s, 9H), 2.20 (s, 9H) . 13C NMR (250 MHz, CDCl3) delta 139.07, 135.46, 130.12, 71.56, 51.04, 20.71., 134030-21-0
The synthetic route of 134030-21-0 has been constantly updated, and we look forward to future research findings.
Reference£º
Article; Musengimana, Eric; Fatakanwa, Claver; Oriental Journal of Chemistry; vol. 29; 4; (2013); p. 1489 – 1496;,
Metal catalyst and ligand design
Ligand Template Strategies for Catalyst Encapsulation – NCBI